Luminescent Control of Milk Freezing during Transportation and Storage

Mihail Belyakov; Igor Efremenkov

doi:10.21603/1019-8946-2024-6-21

UDC 63

LUMINESCENT CONTROL OF MILK FREEZING DURING TRANSPORTATION AND STORAGE Luminescent Control of Milk Freezing during Transportation and Storage

АА Аа

Published in Dairy industry · Pages 16–20 · Rubric: Research Article

DOI: https://doi.org/10.21603/1019-8946-2024-6-21

Received: 20.05.2024 Accepted: 01.12.2024 Published: 23.12.2024 Language of publication: RUS

Authors

Mihail Belyakov

SPIN

Igor Efremenkov

SPIN

Mihail Belyakov

Academic degree: doctor of technical sciences

Federal Scientific Agroengineering Center VIM Russian Federation · Moscow

SPIN

Igor Efremenkov

Federal Scientific Agroengineering Center VIM Russian Federation · Moscow

SPIN

ABSTRACT

Optical monitoring improves the efficiency of milk storage and transportation. For instance, optical photoluminescent diagnostics can be used to determine accidental freezing of milk caused by inappropriate storage and transportation. This research featured milk of Michurino brand with 3.2% fat. Its parameters were monitored using an Expert Profi ultrasonic analyzer. The optical diagnostics involved a CM2203 diffraction spectrofluorimeter. After temporary defrosting, the milk quality deteriorated. The spectral characteristics of the previously frozen sample and the control demonstrated quantitative differences in the range of 300–400 nm. Differences also occurred at excitation wavelengths of 324 nm and 360 nm while the excitation wavelengths of 290 nm and 445 nm did not react to freezing. Integral photoluminescence flux Φ324 in the sample subjected to temporary freezing exceeded the same indicator in the unfrozen sample by 12.5% whereas fluxes Φ445 remained almost the same. These differences made it possible to develop an express method for detecting milk freezing. It included excitation with 324 nm (working xcitation) and 445 nm (reference excitation), registration of photoluminescent radiation at 360–600 nm and 480–660 nm, and calculation of the Φ324 vs. Φ445 ratio. The method may be used with LEDs or photodiodes for a non-destructive express monitoring of milk during its storage and transportation in cold regions.

KEYWORDS

optical diagnostics, milk, transportation, luminescence, freezing, storage, spectral analysis

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Belyakov M. B., Efremenkov I. Y. Luminescent Control of Milk Freezing during Transportation and Storage // Dairy industry. 2024. no. 6. pp. 16-20. DOI: https://doi.org/10.21603/1019-8946-2024-6-21. (Date of access 17.09.2026).

MLA

Mihail Belyakov, Efremenkov I. Y.. "Luminescent Control of Milk Freezing during Transportation and Storage." Dairy industry.6 (2024): 16-20. DOI: https://doi.org/10.21603/1019-8946-2024-6-21.

APA

Belyakov M. B., Efremenkov I. Y. (2024). Luminescent Control of Milk Freezing during Transportation and Storage. Dairy industry(6), 16-20. https://doi.org/10.21603/1019-8946-2024-6-21

Chicago

Mihail Belyakov, Efremenkov I. Y.. "Luminescent Control of Milk Freezing during Transportation and Storage." Dairy industry, no. 6 (2024): 16-20. https://doi.org/10.21603/1019-8946-2024-6-21.

WIKI

{{cite journal | author = Belyakov M. B., Efremenkov I. Y. | title = Luminescent Control of Milk Freezing during Transportation and Storage | journal = Dairy industry | year = 2024 | issue = 6 | pages = 16-20 | doi = 10.21603/1019-8946-2024-6-21 }}

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LUMINESCENT CONTROL OF MILK FREEZING DURING TRANSPORTATION AND STORAGE Luminescent Control of Milk Freezing during Transportation and Storage

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